Ammonium formate → HCID 89725915, compound

Participants

Reaction Steps

Under a nitrogen atmosphere combine 4-benzyl-2-(2-isopropoxyphenyl)morpholine (0.51 g, 2 mmol), 10% PdOH/Carbon (0.51 g, 10 mol %) and anhydrous ammonium formate (0.53 g, 10 mmol). Heat the resulting mixture to reflux and stir. Monitor the progress of the reaction via thin layer chromatography. After completion, filter reaction mixture through a pad of Celite®; collect the filtrate; and remove the solvent under reduced pressure to give the title compound as an oil (0.25 g, 63%). MS (m/z): 433 (M+1).

Provenance & Evidence