huagongshe.com
HRID880375

反应详情

EQUATION

反应方程式

HRID 880375 的结构方程式

REACTANTS

反应物

4
结构：O=C([O-])[O-].[Na+].[Na+]
HCID10340

Carbonic acid sodium salt (1:2)

CNa2O3

结构：CC1(C)OB(c2ccccc2C#N)OC1(C)C
HCID3570229

2-(4,4,5,5-Tetramethyl-1,3,2-dioxaborolan-2-yl)benzonitrile

C13H16BNO2

结构：CC#N.O
HCID18373917

Acetonitrile--water (1/1)

C2H5NO

结构：CC(c1ccccc1)n1ncc(Cl)c(Cl)c1=O
HCID68013986

未命名化合物

PRODUCTS

生成物

1
结构：CC(c1ccccc1)n1ncc(-c2ccccc2C#N)c(-c2ccccc2C#N)c1=O
HCID57385631

未命名化合物

收率 3.4%

AUXILIARIES

试剂、催化剂与溶剂

1
结构：[Cl][Pd][Cl]
催化剂HCID24290

未命名化合物

PROCEDURE

实验过程

Compound 4 is prepared from the intermediate 1a and 2-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)benzonitrile according to step 1 of the method of synthesis using PdCl2/2PPh3, Na2CO3 and a mixture of water/acetonitrile: 1/1. The minor product formed corresponds to compound 4 (yield: 3.4%).