HCID 86654673, compound → HCID 66914943, compound

Participants

Reaction Steps

10% Palladium-carbon (100 mg) was added to a solution of 1-(2-azidoethyl)-2-methyl-4-phenyl-pyrrole (640 mg, 2.96 mmol) in methanol (20 mL) at room temperature and hydrogenated at atmospheric pressure for 27 h. The catalyst was filtered and washed with methanol (20 mL). The combined filtrate and washings were concentrated in vacuo to afford 2-(2-methyl-4-phenyl-pyrrol-1-yl)ethanamine (490 mg, 83%) as a brown syrup.

Provenance & Evidence