HuagongsheHuagongshe Chemistry Print Report · For research reference only
3-Methoxyaniline → 2'-Amino-3'-methyl-4'-methoxyacetophenone
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 3-Methoxyaniline | HCID 10824 | — |
| Reactant | 3-Methoxy-2-methylaniline | HCID 11804822 | — |
| Product | 2'-Amino-3'-methyl-4'-methoxyacetophenone | HCID 25067316 | 23% |
Reaction Steps
1-(2-Amino-3-methyl-4-methoxyphenyl)ethanone 201b was synthesized from 3-methoxy-2-methylaniline 215b as a yellow solid in 23% yield, according to the procedure as described for compound 215a. MS (ESI, EI+): m/z=180 (MH+).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08993595B2 |
| Source dataset | uspto-grants-2015_03 |
| ORD ID | ord-194f4cd23e6449a79ac3e37b6090f49d |
| Source note | uspto-grants-2015_03 |