Decanoic Acid → HCID 22239422, compound

HRID 882214Notes

Reaction equation

HRID 882214 reaction equation
[OH:1][C:2]([CH2:4][CH2:5][CH2:6][CH2:7][CH2:8][CH2:9][CH2:10][CH2:11][CH3:12])=[O:3].[OH-].[K+]>O>[C:2]([O-:3])(=[O:1])[CH2:4][CH2:5][CH2:6][CH2:7][CH2:8][CH2:9][CH3:10].[O-:3][C:2]([CH2:4][CH2:5][CH2:6][CH2:7][CH2:8][CH2:9][CH2:10][CH2:11][CH3:12])=[O:1]

Participants

4

Reactant 2

HCID 2969Decanoic AcidHCID 14797Potassium Hydroxide

Product 1

HCID 22239422HCID 22239422, compound

Reagents, catalysts & solvents 1

HCID 962WaterSolvent

Procedure

While introducing nitrogen, 280 g of polyglycerol (hydroxyl number=1104 mg KOH/g) and 70.0 g of caprylic/capric acid (acid number=361 mg KOH/g) were stirred at 240° C. until an acid number of 0.5 mg KOH/g was reached. The water formed in the course of the reaction was distilled off continuously. After cooling to room temperature, the reaction product was in the form of a clear liquid.

Workup

  1. distillationwas distilled off continuously

Sources & evidence

ORD record
ord-a25d10b9fc58463fa7012177ab9c6e8c
Source dataset
uspto-grants-2015_03
Patent number
US08993792B2

Reaction notes

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