Decanoic Acid → HCID 22239422, compound

HRID 882215Notes

Reaction equation

HRID 882215 reaction equation
[OH:1][C:2]([CH2:4][CH2:5][CH2:6][CH2:7][CH2:8][CH2:9][CH2:10][CH2:11][CH3:12])=[O:3].[OH-].[K+]>O>[C:2]([O-:3])(=[O:1])[CH2:4][CH2:5][CH2:6][CH2:7][CH2:8][CH2:9][CH3:10].[O-:3][C:2]([CH2:4][CH2:5][CH2:6][CH2:7][CH2:8][CH2:9][CH2:10][CH2:11][CH3:12])=[O:1]

Participants

4

Reactant 2

HCID 2969Decanoic AcidHCID 14797Potassium Hydroxide

Product 1

HCID 22239422HCID 22239422, compound

Reagents, catalysts & solvents 1

HCID 962WaterSolvent

Procedure

While introducing nitrogen, 144 g of polyglycerol (hydroxyl number 32 1113 mg KOH/g) and 36.0 g caprylic/capric acid (acid number=355 mg KOH/g) was stirred at 210° C. until an acid number of 1.0 mg KOH/g was reached. The water formed in the course of the reaction was distilled off continuously. After cooling to room temperature, the reaction product was in the form of a clear liquid.

Workup

  1. distillationwas distilled off continuously

Sources & evidence

ORD record
ord-bfd33592442f497ea6695af82ff00e5c
Source dataset
uspto-grants-2015_03
Patent number
US08993792B2

Reaction notes

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