Calcium Hydroxide → HCID 16679760, compound

HRID 882327Notes

Reaction equation

HRID 882327 reaction equation
[C:1]([S:5][CH2:6][C:7]1([CH3:14])[NH:11][C:10](=[O:12])[NH:9][C:8]1=[O:13])([CH3:4])([CH3:3])[CH3:2].[OH-:15].[Ca+2].[OH-]>O>[C:10]([NH:11][C@:7]([CH3:14])([C:8]([OH:15])=[O:13])[CH2:6][S:5][C:1]([CH3:4])([CH3:3])[CH3:2])(=[O:12])[NH2:9]

Participants

4

Reactant 2

HCID 6093208Calcium HydroxideHCID 11195294HCID 11195294, compound

Product 1

HCID 16679760HCID 16679760, compoundYield 25%

Reagents, catalysts & solvents 1

HCID 962WaterSolvent

Conditions

Temperature
100 °C

Procedure

First, 5-tert-butylthiomethyl-5-methylhydantoin (purity content 10.82 g, 50.0 mmol) was mixed with calcium hydroxide (3.70 g, 50.0 mmol), and water (60 g), and the mixture was heated to 100° C. and stirred for 3.5 hours. The HPLC analysis of the reaction solution showed the production of the title compound in a reaction yield of 25%.

Sources & evidence

ORD record
ord-bd2d092dee364e3597f51194af47270f
Source dataset
uspto-grants-2015_03
Patent number
US08993800B2

Reaction notes

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