1-Bromopentane → 2-(3-(3-(Pentyloxy)phenyl)propyl)isoindoline-1,3-dione

참여 물질

역할	이름	HCID	투입량
반응물	1-Bromopentane	HCID 8057	—
반응물	2-[3-(3-Hydroxyphenyl)propyl]isoindole-1,3-dione	HCID 58027542	—
생성물	2-(3-(3-(Pentyloxy)phenyl)propyl)isoindoline-1,3-dione	HCID 67315464	—

반응 단계

Alkylation reaction of phenol 58 with pentyl bromide gave 2-(3-(3-(pentyloxy)phenyl)propyl)isoindoline-1,3-dione as yellow oil. Yield (0.549 g, 46%): 1H NMR (400 MHz, CDCl3) δ 7.81-7.84 (m, 2H), 7.69-7.72 (m, 2H), 7.11-7.16 (m, 1H), 6.76 (d, J=7.6 Hz, 1H), 6.73 (s, 1H), 6.66 (dd, J=7.8, 2.2 Hz, 1H), 3.91 (t, J=6.8 Hz, 2H), 3.74 (t, J=7.2 Hz, 2H), 2.65 (t, J=7.6 Hz, 2H), 2.01-2.07 (m, 2H), 1.73-1.78 (m, 2H), 1.34-1.48 (m, 4H), 0.92 (t, J=7.2 Hz, 3H).

출처 및 근거

DOI	10.6084/m9.figshare.5104873.v1
특허 번호	US08993807B2
출처 데이터셋	uspto-grants-2015_03
ORD ID	ord-ed584f49c0a94670840aae9caa5c5b0e
출처 메모	uspto-grants-2015_03