HuagongsheHuagongshe Chemistry Print Report · For research reference only
Triacetoxyperiodinane → HCID 66644662, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Triacetoxyperiodinane | HCID 159087 | — |
| Reactant | Nitrate(1-), oxo- | HCID 3001380 | — |
| Reactant | 3-Amino-2-hydroxy-4-phenylbutanamide | HCID 13882355 | — |
| Reactant | HCID 42127375 | HCID 42127375 | — |
| Reactant | HCID 178514248 | HCID 178514248 | — |
| Product | HCID 66644662 | HCID 66644662 | — |
Reaction Steps
Coupling of (R)-5-oxo-1-pyridin-4-ylmethyl-pyrrolidine-2-carboxylic acid with 3-amino-2-hydroxy-4-phenylbutanamide and oxidation of the resulting hydroxyamide intermediate to the corresponding ketoamide using Dess Martin reagent.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08236798B2 |
| Source dataset | uspto-grants-2012_08 |
| ORD ID | ord-eba976035cf342f7a9db16e4644a2ba1 |
| Source note | uspto-grants-2012_08 |