tert-Butyl methacrylate → HCID 68665637, compound

HRID 883072Notes

Reaction equation

HRID 883072 reaction equation
Br[C:2]1[CH:3]=[CH:4][C:5]([O:24][C:25]([F:28])([F:27])[F:26])=[C:6]([C:8]2[CH:17]=[C:16]3[C:11]([C:12]([CH3:22])([CH3:21])[CH2:13][C:14](=[O:20])[N:15]3[CH2:18][CH3:19])=[CH:10][C:9]=2[CH3:23])[CH:7]=1.[C:29]([O:34][C:35]([CH3:38])([CH3:37])[CH3:36])(=[O:33])[C:30]([CH3:32])=[CH2:31]>>[C:35]([O:34][C:29](=[O:33])[C:30]([CH3:32])=[CH:31][C:2]1[CH:3]=[CH:4][C:5]([O:24][C:25]([F:28])([F:26])[F:27])=[C:6]([C:8]2[CH:17]=[C:16]3[C:11]([C:12]([CH3:22])([CH3:21])[CH2:13][C:14](=[O:20])[N:15]3[CH2:18][CH3:19])=[CH:10][C:9]=2[CH3:23])[CH:7]=1)([CH3:38])([CH3:37])[CH3:36]

Participants

3

Reactant 2

HCID 11448tert-Butyl methacrylateHCID 68666441HCID 68666441, compound

Product 1

HCID 68665637HCID 68665637, compound

Procedure

Compound 9C was prepared form Compound 9B using a procedure similar to that described for Example 5C, except that t-butyl methacrylate was used as the coupling reagent. MS (electrospray): mass calculated for C26H28F3NO4, 475.20; m/z found, 476.2[M+H]+.

Sources & evidence

ORD record
ord-3a631023f9414ed5bc02f9b05851f774
Source dataset
uspto-grants-2012_08
Patent number
US08236819B2

Reaction notes

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