2-Methoxyphenylboronic acid → HCID 68667046, compound

HRID 883076Notes

Reaction equation

HRID 883076 reaction equation
Br[C:2]1[CH:11]=[C:10]2[C:5]([C:6]([CH3:16])([CH3:15])[CH2:7][C:8](=[O:14])[N:9]2[CH2:12][CH3:13])=[CH:4][C:3]=1[CH3:17].[CH3:18][O:19][C:20]1[CH:25]=[CH:24][CH:23]=[CH:22][C:21]=1B(O)O>>[CH2:12]([N:9]1[C:10]2[C:5](=[CH:4][C:3]([CH3:17])=[C:2]([C:21]3[CH:22]=[CH:23][CH:24]=[CH:25][C:20]=3[O:19][CH3:18])[CH:11]=2)[C:6]([CH3:16])([CH3:15])[CH2:7][C:8]1=[O:14])[CH3:13]

Participants

3

Reactant 2

HCID 27339582-Methoxyphenylboronic acidHCID 219664867-Bromo-1-ethyl-4,4,6-trimethyl-3,4-dihydro-1H-quinolin-2-one

Product 1

HCID 68667046HCID 68667046, compound

Procedure

Compound 39A was prepared from Compound 1A using a procedure similar to that described in Example 1B, except using 2-methoxy phenylboronic acid as the starting material. MS (electrospray): mass calculated for C21H25NO2, 323.19; m/z found 324.2 [M+H]+.

Sources & evidence

ORD record
ord-e428108a7de640edbbc308ae77607b3b
Source dataset
uspto-grants-2012_08
Patent number
US08236819B2

Reaction notes

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