HuagongsheHuagongshe Chemistry Print Report · For research reference only
1-(2-Fluorophenyl)piperazine → HCID 68560530, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 1-(2-Fluorophenyl)piperazine | HCID 70529 | — |
| Reactant | Diisopropylethylamine | HCID 81531 | — |
| Reactant | Sodium triacetoxyborohydride | HCID 5049666 | — |
| Reactant | HCID 86639928 | HCID 86639928 | — |
| Product | HCID 68560530 | HCID 68560530 | — |
Reaction Steps
53 mg (98%) of target compound was obtained by using a method same as in Example 1 by using 3-(1-phenyl-3-ethyl-1H-pyrazol-5-yl)propanal (31 mg, 0.138 mmol), 1-(2-fluorophenyl)piperazine (28 mg, 0.154 mmol), DIPEA (0.036 mL, 0.206 mmol) and NaBH(OAc)3 (89 mg, 0.418 mmol).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08236806B2 |
| Source dataset | uspto-grants-2012_08 |
| ORD ID | ord-762d09acae1243899d24dbf236efeb82 |
| Source note | uspto-grants-2012_08 |