HuagongsheHuagongshe Chemistry Print Report · For research reference only
Triethyl phosphite → HCID 58019379, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Triethyl phosphite | HCID 31215 | — |
| Reactant | 2,5-Bis(chloromethyl)-2',5'-dimethyl-1,1'-biphenyl | HCID 22146228 | — |
| Product | HCID 58019379 | HCID 58019379 | — |
Reaction Steps
50 g (180 mmol) of 2′,5′-bis-chloromethyl-2,5-dimethylbiphenyl are heated at 160° C. in 63 ml (366 mmol) of triethyl phosphite until the evolution of gas is complete. The residue which remains is employed in the subsequent reaction without further purification.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08236968B2 |
| Source dataset | uspto-grants-2012_08 |
| ORD ID | ord-b1d82dee62014dc896a47d3c3e255574 |
| Source note | uspto-grants-2012_08 |