HuagongsheHuagongshe Chemistry Print Report · For research reference only
Stannous Chloride → 4-(2-Amino-4-methyl-phenylsulfanyl)-phenol
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Stannous Chloride | HCID 24479 | — |
| Reactant | 4-(4-Methyl-2-nitro-phenylsulfanyl)-phenol | HCID 54911098 | — |
| Product | 4-(2-Amino-4-methyl-phenylsulfanyl)-phenol | HCID 66808123 | 117.5% |
Reaction Steps
The product from Example 9b (8.65 g, 31.3 mmol) was reduced with SnCl2 following the procedure from Example 7f giving the title compound as a white solid (8.51 g, 100%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08236950B2 |
| Source dataset | uspto-grants-2012_08 |
| ORD ID | ord-620b2d4a12d74910a5b44de5d984cdf9 |
| Source note | uspto-grants-2012_08 |