HuagongsheHuagongshe Chemistry Print Report · For research reference only
Stannous Chloride → 4-(2-amino-4-chlorophenoxy)-N-(2-methoxyethyl)benzamide
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Stannous Chloride | HCID 24479 | — |
| Reactant | 4-(4-chloro-2-nitrophenoxy)-N-(2-methoxyethyl)benzamide | HCID 25931314 | — |
| Product | 4-(2-amino-4-chlorophenoxy)-N-(2-methoxyethyl)benzamide | HCID 67249338 | 100% |
Reaction Steps
The product from Example 34d (1.0 g, 2.85 mmol) was reduced with SnCl2 following the procedure from Example 7f giving the title compound as a clear oil (900 mg, 100%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08236950B2 |
| Source dataset | uspto-grants-2012_08 |
| ORD ID | ord-9b8e49783a964d079e7dc380c66fdd84 |
| Source note | uspto-grants-2012_08 |