4-Chloro-3-nitrophenol → HCID 59368060, compound

HRID 883928Notes

Reaction equation

HRID 883928 reaction equation
[Cl:1][C:2]1[CH:7]=[C:6]([F:8])[C:5]([N+:9]([O-:11])=[O:10])=[CH:4][C:3]=1[OH:12].Cl[CH2:14][C:15]1[CH:20]=[CH:19][C:18](OC)=[CH:17][CH:16]=1.ClC1C=CC(O)=CC=1[N+]([O-])=O>>[CH2:14]([O:12][C:3]1[CH:4]=[C:5]([N+:9]([O-:11])=[O:10])[C:6]([F:8])=[CH:7][C:2]=1[Cl:1])[C:15]1[CH:20]=[CH:19][CH:18]=[CH:17][CH:16]=1

Participants

4

Reactant 3

HCID 691274-Chloro-3-nitrophenolHCID 699934-Methyloxybenzyl chlorideHCID 158655Phenol, 2-chloro-4-fluoro-5-nitro-

Product 1

HCID 59368060HCID 59368060, compound

Procedure

The title compound was prepared according to the procedure of Example 10C substituting benzyl bromide and the product from Example 47C for 1-chloromethyl-4-methoxy-benzene and 4-chloro-3-nitro-phenol (0.72 g, 79%).

Sources & evidence

ORD record
ord-7b290a65fa3341dca9f2330ac5de2887
Source dataset
uspto-grants-2012_08
Patent number
US08236950B2

Reaction notes

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