HuagongsheHuagongshe Chemistry Print Report · For research reference only
Acryloyl chloride → 3-Acrylamidophenylboronic acid
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Acryloyl chloride | HCID 13140 | — |
| Reactant | 3-Aminophenylboronic acid | HCID 92269 | — |
| Product | 3-Acrylamidophenylboronic acid | HCID 10321331 | — |
Reaction Steps
3-Acrylamido-phenylboronic acid (“3-APB”) was synthesised by reacting 3-amino phenylboronic acid with an excess of acryloyl chloride in an aqueous alkaline solution. The product was extracted in acetone and dried using a rotary evaporator. The structure of 3-APB was confirmed using NMR. The purity was about 90%, TLC showing very little contamination.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08241574B2 |
| Source dataset | uspto-grants-2012_08 |
| ORD ID | ord-388bda6ba2de4b31a381f4a1d3373c80 |
| Source note | uspto-grants-2012_08 |