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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 884361Generated: October 31, 2026

Hydrogen Peroxide → HCID 58109268, compound

https://huagongshe.com/reaction/884361

Reaction equation

Participants

RoleNameHCIDCharge
ReactantHydrogen PeroxideHCID 784—
ReactantSodium HydroxideHCID 14798—
ReactantHCID 58109481HCID 58109481—
SolventTetrahydrofuranHCID 8028—
ProductHCID 58109268HCID 58109268—

Reaction Steps

The two diastereomers of (3S)-tert-butyl 3-(6-(4-fluorophenyl)-6-(3-hydroxypropyl)-2-oxo-1,3-oxazinan-3-yl)piperidine-1-carboxylate were prepared from (3S)-tert-butyl 3-(6-allyl-6-(4-fluorophenyl)-2-oxo-1,3-oxazinan-3-yl)piperidine-1-carboxylate by treatment with (i) BH3 in THF and (ii) H2O2 and NaOH.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS08242111B2
Source datasetuspto-grants-2012_08
ORD IDord-2a84eb97c2cf49e5ad687037610be3ec
Source noteuspto-grants-2012_08