Hydrogen Peroxide → HCID 68260485, compound

Participants

Reaction Steps

A solution of 576 mg of selenyl ether 171 (1.22 mmol) in 15 ml of anhydrous CH2Cl2 was cooled to 0° C., added with 0.4 ml of pyridine and 0.8 ml H2O2 (30%) and stirred overnight. The intensely orange-colored solution was subsequently concentrated and purified using silica gel column chromatography (CH2Cl2) to obtain 312 mg of vinylproline 172 (1.16 mmol, 95%) as a yellowish oil.

Provenance & Evidence