Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
2-Nitro-4-(trifluoromethoxy)phenol → 2-Amino-4-(trifluoromethoxy)phenol
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | 2-Nitro-4-(trifluoromethoxy)phenol | HCID 2775775 | — |
| 반응물 | HCID 178418361 | HCID 178418361 | — |
| 촉매 | Palladium | HCID 23938 | — |
| 용매 | Ethyl Acetate | HCID 8857 | — |
| 생성물 | 2-Amino-4-(trifluoromethoxy)phenol | HCID 2737729 | 100% |
반응 단계
A mixture of 4.53 g of 4-trifluoromethoxy-2-nitrophenol, 35 ml of ethyl acetate and 1.0 g of 5% palladium on carbon was stirred under about one atmosphere of hydrogen at room temperature for 1.7 hours. The mixture was filtered through Celite™. The filtrate was concentrated under reduced pressure to give 3.92 g of 2-amino-4-trifluoromethoxy phenol.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US08242133B2 |
| 출처 데이터셋 | uspto-grants-2012_08 |
| ORD ID | ord-0ea26df9fb9049beb4359c0ae80fc46e |
| 출처 메모 | uspto-grants-2012_08 |