Phosphorus tribromide → HCID 58237481, compound

HRID 885366Notes

Reaction equation

HRID 885366 reaction equation
[CH3:1][O:2][C:3](=[O:23])[CH2:4][C:5]1[CH:10]=[CH:9][C:8]([O:11][CH3:12])=[C:7]([O:13][C:14]2[CH:19]=[C:18]([Br:20])[CH:17]=[CH:16][C:15]=2[CH2:21]O)[CH:6]=1.P(Br)(Br)[Br:25]>>[CH3:1][O:2][C:3](=[O:23])[CH2:4][C:5]1[CH:10]=[CH:9][C:8]([O:11][CH3:12])=[C:7]([O:13][C:14]2[CH:19]=[C:18]([Br:20])[CH:17]=[CH:16][C:15]=2[CH2:21][Br:25])[CH:6]=1

Participants

3

Reactant 2

HCID 24614Phosphorus tribromideHCID 58237664HCID 58237664, compound

Product 1

HCID 58237481HCID 58237481, compound

Procedure

Prepared according to the procedure described in Example 6, Step 4, using the following starting materials: [3-(5-bromo-2-hydroxymethyl-phenoxy)-4-methoxy-phenyl]-acetic acid methyl ester and phosphorus tribromide.

Workup

  1. customPrepared

Sources & evidence

ORD record
ord-58f5383903954aa697bc2c0919cc941b
Source dataset
uspto-grants-2012_08
Patent number
US08242145B2

Reaction notes

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