HuagongsheHuagongshe Chemistry Print Report · For research reference only
1-(4-Phenylbutoxy)hept-6-en-3-ol → 1-(4-Phenylbutoxy)hept-6-en-3-one
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 1-(4-Phenylbutoxy)hept-6-en-3-ol | HCID 67244432 | — |
| Reactant | 3-(4-Phenylbutoxy)propionaldehyde | HCID 86658307 | — |
| Product | 1-(4-Phenylbutoxy)hept-6-en-3-one | HCID 67246223 | 88.6% |
Reaction Steps
Obtained from Intermediate 14 (0.41 g, 1.56 mmol) by the procedure described for the Intermediate 13. Purification by column chromatography with silica gel and methylene chloride/acetone (20:1) as eluent gave the title compound (0.36 g, 88%) as oil.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08242177B2 |
| Source dataset | uspto-grants-2012_08 |
| ORD ID | ord-3833f2ff588146258ed464e519f79028 |
| Source note | uspto-grants-2012_08 |