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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 885550Generated: October 31, 2026

HCID 67245149, compound → HCID 67245686, compound

https://huagongshe.com/reaction/885550

Reaction equation

Participants

RoleNameHCIDCharge
ReactantHCID 67245149HCID 67245149—
CatalystPalladiumHCID 23938—
SolventEthanolHCID 702—
ProductHCID 67245686HCID 6724568696.4%

Reaction Steps

To a solution of Intermediate 61 (2.52 g, 5.65 mmol) in ethanol (120 mL) was added palladium on charcoal (300 mg). The mixture was bidrogenated at 40 psi for 4 hours. The catalyst was filtered through Celite and the solvent removed under pressure to give the title compound (1.94 g, 96%) as oil.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS08242177B2
Source datasetuspto-grants-2012_08
ORD IDord-8e14b6fb7b4d4c65a90d1a47812160b5
Source noteuspto-grants-2012_08