HuagongsheHuagongshe Chemistry Print Report · For research reference only
Methyl chloroformate → methyl N-methyl-N-(4-nitrophenyl)carbamate
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Methyl chloroformate | HCID 6586 | — |
| Reactant | N-Methyl-4-nitroaniline | HCID 7483 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | methyl N-methyl-N-(4-nitrophenyl)carbamate | HCID 610793 | — |
Reaction Steps
The title compound was prepared from N-methyl-4-nitroaniline and methyl chloroformate according to Method Y and was isolated as a pale yellow solid (84%) after trituration in cold MeOH. δH (DMSO-d6) 8.22 (2H, d, J 9.3 Hz), 7.64 (2H, d, J 9.3 Hz), 3.70 (3H, s), 3.32 (3H, s).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08242116B2 |
| Source dataset | uspto-grants-2012_08 |
| ORD ID | ord-29310bcaca1442a0a8380884526ce804 |
| Source note | uspto-grants-2012_08 |