HCID 68577895, compound → HCID 68579396, compound

Participants

Reaction Steps

A mixture of tert-butyl 9-(cyclohexa-1-en-1-yl)-2,3-dihydro-1,4-benzoxazepine-4(5H)-carboxylate (160 mg, 0.486 mmol) and 10% palladium on carbon (100 mg) in methanol (5 ml) was stirred under a hydrogen atmosphere for 12 hr. The reaction mixture was filtered, and the filtrate was concentrated to give the desired product (150 mg, 93.2%) as an oil.

Provenance & Evidence