HuagongsheHuagongshe Chemistry Print Report · For research reference only
Benzylamine → HCID 178442043, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Benzylamine | HCID 7504 | — |
| Reactant | Acetonitrile--water (1/1) | HCID 18373917 | — |
| Reactant | HCID 178442045 | HCID 178442045 | — |
| Solvent | Dimethylformamide | HCID 6228 | — |
| Product | HCID 178442043 | HCID 178442043 | — |
Reaction Steps
Twenty (20) mg (37.1 μmol) fredericamycin are dissolved in 1 ml DMF under argon, then 4.76 mg (44.50 μmol) benzylamine are added at room temperature. According to HPLC (RP18, acetonitrile/water), a homogenous new product has formed after 3 h. The reaction mixture is concentrated at high vacuum until dry.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08247424B2 |
| Source dataset | uspto-grants-2012_08 |
| ORD ID | ord-2032a8d3d5624acdb9ec33c71b557392 |
| Source note | uspto-grants-2012_08 |