HCID 68700385, compound → HCID 25024912, compound

Participants

Reaction Steps

To a solution of N-[2-(2-methyl-6,7-dihydrocyclopenta[e]indazol-8(2H)-ylidene)ethyl]propanamide (83 mg, 0.225 mmol) in methanol (2 mL) was added palladium-carbon powder (8 mg), and the mixture was stirred under a hydrogen atmosphere at room temperature for 3 hr. The catalyst was filtered off, and the filtrate was concentrated under reduced pressure and purified by thin layer chromatography (methanol/ethyl acetate=10/90) to give the title compound (45.1 mg, yield 74%).

Provenance & Evidence