2-Chloro-5-nitroaniline → HCID 3498511, compound

Participants

Reaction Steps

2-Chloro-5-nitroaniline (3.36 g) was dissolved in CH2Cl2 (45 mL) at 0° C. and pivaloyl chloride (1.99 mL) was added dropwise followed by TEA (4.06 mL). The mixture was stirred at RT for 2 days and a solid precipitated. Solid was filtered, rinsed with MeOH. Mother liquid was evaporated, solid was filtered on silica pad and solvent evaporated. Combined white solids were dried.

Provenance & Evidence