HuagongsheHuagongshe Chemistry Print Report · For research reference only
2-Bromo-6-methoxynaphthalene → HCID 58488023, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2-Bromo-6-methoxynaphthalene | HCID 78786 | — |
| Reactant | HCID 58487948 | HCID 58487948 | — |
| Product | HCID 58488023 | HCID 58488023 | — |
Reaction Steps
The title compound was prepared following the procedure of Intermediate 17, but starting from 2-bromo-6-methoxynaphthalene. Purification by chromatography (DCM/MeOH 80/20) afforded the title compound as an off white solid (43%). HPLC (Condition A), Rt: 2.2 min (HPLC purity: 98.4%). M+(ESI): 257.2
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08247437B2 |
| Source dataset | uspto-grants-2012_08 |
| ORD ID | ord-cf97c35a042c4db4b65b26fb42487abe |
| Source note | uspto-grants-2012_08 |