huagongshe.com
HRID888196

反应详情

EQUATION

反应方程式

HRID 888196 的结构方程式

REACTANTS

反应物

2
结构：COc1ccc(Br)cc1
HCID7730

Benzene, 1-bromo-4-methoxy-

C7H7BrO

结构：COc1ccc(N2CCN[C@H](C)C2)cc1OC
HCID58487959

未命名化合物

PRODUCTS

生成物

1
结构：COc1ccc(N2CCN[C@H](C)C2)cc1
HCID27441151

未命名化合物

PROCEDURE

实验过程

The title compound was prepared following the procedure of Intermediate 25, but starting from 1-bromo-4-methoxybenzene. Purification by flash chromatography (CHCl3/MeOH) gave the title compound as a yellow oil. M+(ESI): 207.2. HPLC (Condition A), Rt: 1.2 min (HPLC purity: 922%).

WORKUP

后处理

  1. customThe title compound was prepared
  2. customPurification by flash chromatography (CHCl3/MeOH)