HuagongsheHuagongshe Chemistry Print Report · For research reference only
3-Isopropenyl-5-(5-methylpyridin-2-yl)benzoic acid → 3-Isopropyl-5-(5-methylpyridin-2-yl)benzoic acid
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 3-Isopropenyl-5-(5-methylpyridin-2-yl)benzoic acid | HCID 68494807 | — |
| Reactant | HCID 178418361 | HCID 178418361 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | 3-Isopropyl-5-(5-methylpyridin-2-yl)benzoic acid | HCID 68496952 | 99.2% |
Reaction Steps
To a solution of 3-isopropenyl-5-(5-methylpyridin-2-yl)benzoic acid (150 mg, 0.592 mmol) in ethanol (11.8 mL) was added 10% palladium on carbon (50.0 mg, 0.047 mmol) and the mixture was placed under 1 atm of hydrogen. After 1 h, filtration and concentration gave the crude title compound (150 mg). MS 256.2 (M+1).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08247401B2 |
| Source dataset | uspto-grants-2012_08 |
| ORD ID | ord-e39aa2da1d1246808d1f71cb8338f589 |
| Source note | uspto-grants-2012_08 |