HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 888483Generated: October 31, 2026
Dichloromethane → HCID 58372719, compound
https://huagongshe.com/reaction/888483
Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | Dichloromethane | HCID 6344 | — |
| Reactant | Stannous Chloride | HCID 24479 | — |
| Reactant | Sodium Bicarbonate | HCID 516892 | — |
| Reactant | HCID 58372772 | HCID 58372772 | — |
| Solvent | Ethanol | HCID 702 | — |
| Solvent | Water | HCID 962 | — |
| Product | HCID 58372719 | HCID 58372719 | — |
Reaction Steps
[4-Methoxy-3-(4-nitro-2-phenylsulfanylmethyl-phenoxy)-phenyl]-acetic acid ethyl ester (0.4 g, 0.9 mmol) and tin(II) chloride (0.6 g, 2.7 mmol) were combined in EtOH (20 mL) and stirred overnight at 70° C. CH2Cl2, H2O, and sodium bicarbonate were added, and the mixture was filtered through. Celite. The organic layer was separated and concentrated to give the title compound.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| Patent number | US08247602B2 |
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| Source dataset | uspto-grants-2012_08 |
|---|
| ORD ID | ord-abafea7bddce4f488218865d393942e3 |
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| Source note | uspto-grants-2012_08 |
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