HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 888709Generated: October 30, 2026
Methyl p-toluenesulfonate → HCID 178503586, compound
https://huagongshe.com/reaction/888709
Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | Methyl p-toluenesulfonate | HCID 6645 | — |
| Reactant | HCID 11263876 | HCID 11263876 | — |
| Solvent | Ethyl Acetate | HCID 8857 | — |
| Product | HCID 178503586 | HCID 178503586 | — |
Reaction Steps
A mixture of 0.127 g of 2-methylthiothiazolo[5,4-c]pyridine (from methylation of thiazolo[5,4-c]pyridine-2(1H)-thione with potassium carbonate and methyl iodide) and 0.143 g methyl tosylate is heated at 120° C. for one hour. Ethyl acetate (8 mL) is added, the mixture is stirred for 30 minutes, and Compound 6 is isolated by suction filtration.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
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| Patent number | US08252530B2 |
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| Source dataset | uspto-grants-2012_08 |
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| ORD ID | ord-cafd5baa6ca040028f000f326e9e9065 |
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| Source note | uspto-grants-2012_08 |
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