反应详情

温度

80 °C

Under an argon atmosphere, a solution of 2-adamantanone (1.00 g, 6.70 mmol) in ethanol (40 mL) was added with benzylcarbazate (1.11 g, 6.70 mmol) at room temperature and the resultant was stirred at 80° C. for 12 hours. The reaction solution was concentrated in vacuo, and benzyl 2-(adamantan-2-ylidene)hydrazinecarboxylate (2.03 g, quant.) was obtained as a white crystalline powder.

1. concentrationThe reaction solution was concentrated in vacuo