HuagongsheHuagongshe Chemistry Print Report · For research reference only
1-(Bromomethyl)-2-(methylsulfanyl)benzene → 4,4-Dimethyl-1-[2-(methylthio)benzyl]-2-(adamantan-2-yl)-1,2-diazetidin-3-one
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 1-(Bromomethyl)-2-(methylsulfanyl)benzene | HCID 21793519 | — |
| Reactant | 2-(Adamantan-2-yl)-4,4-dimethyl-1,2-diazetidin-3-one | HCID 67302882 | — |
| Product | 4,4-Dimethyl-1-[2-(methylthio)benzyl]-2-(adamantan-2-yl)-1,2-diazetidin-3-one | HCID 67302714 | — |
Reaction Steps
2-(Adamantan-2-yl)-4,4-dimethyl-1,2-diazetidin-3-one and 2-(methylthio)benzyl bromide were used for a similar reaction and treatment as Process 6 of Example 1, and the title compound was obtained as a white crystalline powder.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08252781B2 |
| Source dataset | uspto-grants-2012_08 |
| ORD ID | ord-3e1afde289b54d7eb99e07f294ebd441 |
| Source note | uspto-grants-2012_08 |