1-(Bromomethyl)-2,3-dichlorobenzene → HCID 67302899, compound
Reaction equation
[CH:1]1([N:8]2[C:11](=[O:12])[C:10]([CH3:14])([CH3:13])[NH:9]2)[CH2:7][CH2:6][CH2:5][CH2:4][CH2:3][CH2:2]1.[Cl:15][C:16]1[C:23]([Cl:24])=[CH:22][CH:21]=[CH:20][C:17]=1[CH2:18]Br>>[CH:1]1([N:8]2[C:11](=[O:12])[C:10]([CH3:14])([CH3:13])[N:9]2[CH2:18][C:17]2[CH:20]=[CH:21][CH:22]=[C:23]([Cl:24])[C:16]=2[Cl:15])[CH2:2][CH2:3][CH2:4][CH2:5][CH2:6][CH2:7]1Participants
3
Procedure
2-Cycloheptyl-4,4-dimethyl-1,2-diazetidin-3-one prepared in Process 4 of Example 83 and 2,3-dichlorobenzyl bromide were used for a similar reaction and treatment as Process 6 of Example 1, and the title compound was obtained as a colorless oil.
Workup
- customwere used for a similar reaction and treatment as Process 6 of Example 1
Sources & evidence
- ORD record
- ord-9d46d8f2623341bf9e35b0989a287ebf
- Source dataset
- uspto-grants-2012_08
- Patent number
- US08252781B2
Reaction notes
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