3-Bromocyclohexene → HCID 46195788, compound

HRID 888851Notes

Reaction equation

HRID 888851 reaction equation
[CH:1]12[CH2:10][CH:5]3[CH2:6][CH:7]([CH2:9][CH:3]([CH2:4]3)[CH:2]1[N:11]1[C:14](=[O:15])[C:13]([CH3:17])([CH3:16])[NH:12]1)[CH2:8]2.Br[CH:19]1[CH2:24][CH2:23][CH2:22][CH:21]=[CH:20]1>>[CH:24]1([N:12]2[C:13]([CH3:17])([CH3:16])[C:14](=[O:15])[N:11]2[CH:2]2[CH:3]3[CH2:4][CH:5]4[CH2:6][CH:7]([CH2:8][CH:1]2[CH2:10]4)[CH2:9]3)[CH2:23][CH2:22][CH2:21][CH:20]=[CH:19]1

Participants

3

Reactant 2

HCID 1370573-BromocyclohexeneHCID 673028822-(Adamantan-2-yl)-4,4-dimethyl-1,2-diazetidin-3-one

Product 1

HCID 46195788HCID 46195788, compound

Procedure

2-(Adamantan-2-yl)-4,4-dimethyl-1,2-diazetidin-3-one prepared in Process 3 of Example 12, and 3-bromocyclohexene were used for a similar reaction and treatment as Process 6 of Example 1, and the title compound was obtained as a colorless oil.

Workup

  1. customwere used for a similar reaction and treatment as Process 6 of Example 1

Sources & evidence

ORD record
ord-4ace9d9376c446d483d918b386b3be45
Source dataset
uspto-grants-2012_08
Patent number
US08252781B2

Reaction notes

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