HCID 46195788, compound → HCID 59361425, compound

Participants

Reaction Steps

A solution of 1-(cyclohexa-2-ene-1-yl)-4,4-dimethyl-2-(adamantan-2-yl)-1,2-diazetidin-3-one (3.20 mg, 0.0100 mmol) in ethanol (2 mL) was added with 10% palladium carbon (catalyst amount), and under hydrogen atmosphere, the resultant was stirred at room temperature for 2 hours. The reaction solution was filtered using celite and concentrated in vacuo. The obtained residue was purified using Preparative Thin-Layer chromatography (hexane:ethyl acetate=3:1), and the title compound (3.2 mg, quant.) was obtained as a colorless oil.

Provenance & Evidence