2-Methylbenzoyl chloride → HCID 46195924, compound

HRID 888856Notes

Reaction equation

HRID 888856 reaction equation
[CH:1]12[CH2:10][CH:5]3[CH2:6][CH:7]([CH2:9][CH:3]([CH2:4]3)[CH:2]1[N:11]1[C:14](=[O:15])[CH:13]([CH:16]([CH3:18])[CH3:17])[NH:12]1)[CH2:8]2.[CH3:19][C:20]1[CH:28]=[CH:27][CH:26]=[CH:25][C:21]=1[C:22](Cl)=[O:23]>>[CH3:19][C:20]1[CH:28]=[CH:27][CH:26]=[CH:25][C:21]=1[C:22]([N:12]1[CH:13]([CH:16]([CH3:18])[CH3:17])[C:14](=[O:15])[N:11]1[CH:2]1[CH:3]2[CH2:4][CH:5]3[CH2:6][CH:7]([CH2:8][CH:1]1[CH2:10]3)[CH2:9]2)=[O:23]

Participants

3

Reactant 2

HCID 702762-Methylbenzoyl chlorideHCID 67303324HCID 67303324, compound

Product 1

HCID 46195924HCID 46195924, compound

Procedure

2-(Adamantan-2-yl)-4-(propan-2-yl)-1,2-diazetidin-3-one prepared in Process 3 of Example 10 and 2-methylbenzoyl chloride were used for a similar reaction and treatment as Example 96, and the title compound was obtained as a colorless oil.

Workup

  1. customwere used for a similar reaction and treatment as Example 96

Sources & evidence

ORD record
ord-729798dd12b741e690ee0de76fdeb1dd
Source dataset
uspto-grants-2012_08
Patent number
US08252781B2

Reaction notes

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