2,4-Dimethylbenzoyl chloride → 2-Cyclohexyl-1-[(2,4-dimethylphenyl)carbonyl]-4,4-dimethyl-1,2-diazetidin-3-one

HRID 888860Notes

Reaction equation

HRID 888860 reaction equation
[CH:1]1([N:7]2[C:10](=[O:11])[C:9]([CH3:13])([CH3:12])[NH:8]2)[CH2:6][CH2:5][CH2:4][CH2:3][CH2:2]1.[CH3:14][C:15]1[CH:23]=[C:22]([CH3:24])[CH:21]=[CH:20][C:16]=1[C:17](Cl)=[O:18]>>[CH:1]1([N:7]2[C:10](=[O:11])[C:9]([CH3:13])([CH3:12])[N:8]2[C:17]([C:16]2[CH:20]=[CH:21][C:22]([CH3:24])=[CH:23][C:15]=2[CH3:14])=[O:18])[CH2:2][CH2:3][CH2:4][CH2:5][CH2:6]1

Participants

3

Reactant 2

HCID 1408672,4-Dimethylbenzoyl chlorideHCID 673030222-Cyclohexyl-4,4-dimethyl-1,2-diazetidin-3-one

Product 1

HCID 593614002-Cyclohexyl-1-[(2,4-dimethylphenyl)carbonyl]-4,4-dimethyl-1,2-diazetidin-3-one

Procedure

2-Cyclohexyl-4,4-dimethyl-1,2-diazetidin-3-one and 2,4-dimethylbenzoyl chloride were used for a similar reaction and treatment as Example 96, and the title compound was obtained as a colorless oil.

Sources & evidence

ORD record
ord-f276a709883b44418faa06310fbac644
Source dataset
uspto-grants-2012_08
Patent number
US08252781B2

Reaction notes

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