Benzoyl chloride, 3-chloro- → 1-[(3-Chlorophenyl)carbonyl]-2-cyclooctyl-4,4-dimethyl-1,2-diazetidin-3-one

HRID 888862Notes

Reaction equation

HRID 888862 reaction equation
[CH:1]1([N:9]2[C:12](=[O:13])[C:11]([CH3:15])([CH3:14])[NH:10]2)[CH2:8][CH2:7][CH2:6][CH2:5][CH2:4][CH2:3][CH2:2]1.[Cl:16][C:17]1[CH:18]=[C:19]([CH:23]=[CH:24][CH:25]=1)[C:20](Cl)=[O:21]>>[Cl:16][C:17]1[CH:18]=[C:19]([C:20]([N:10]2[C:11]([CH3:15])([CH3:14])[C:12](=[O:13])[N:9]2[CH:1]2[CH2:8][CH2:7][CH2:6][CH2:5][CH2:4][CH2:3][CH2:2]2)=[O:21])[CH:23]=[CH:24][CH:25]=1

Participants

3

Reactant 2

HCID 69252Benzoyl chloride, 3-chloro-HCID 673029832-Cyclooctyl-4,4-dimethyl-1,2-diazetidin-3-one

Product 1

HCID 593614551-[(3-Chlorophenyl)carbonyl]-2-cyclooctyl-4,4-dimethyl-1,2-diazetidin-3-one

Procedure

2-Cyclooctyl-4,4-dimethyl-1,2-diazetidin-3-one prepared in Process 5 of Example 73 and 3-chlorobenzoyl chloride were used for a similar reaction and treatment as Example 96, and the title compound was obtained as a white crystalline powder.

Workup

  1. customwere used for a similar reaction and treatment as Example 96

Sources & evidence

ORD record
ord-c1b90b393d764041943e2ed9be00e2d3
Source dataset
uspto-grants-2012_08
Patent number
US08252781B2

Reaction notes

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