o-Toluenesulfonyl chloride → HCID 59361407, compound

HRID 888871Notes

Reaction equation

HRID 888871 reaction equation
[CH:1]12[CH2:10][CH:5]3[CH2:6][CH:7]([CH2:9][CH:3]([CH2:4]3)[CH:2]1[N:11]1[C:14](=[O:15])[C:13]([CH3:17])([CH3:16])[NH:12]1)[CH2:8]2.[C:18]1([CH3:28])[C:19]([S:24](Cl)(=[O:26])=[O:25])=[CH:20][CH:21]=[CH:22][CH:23]=1>>[CH3:16][C:13]1([CH3:17])[N:12]([S:24]([C:19]2[CH:20]=[CH:21][CH:22]=[CH:23][C:18]=2[CH3:28])(=[O:26])=[O:25])[N:11]([CH:2]2[CH:3]3[CH2:4][CH:5]4[CH2:6][CH:7]([CH2:8][CH:1]2[CH2:10]4)[CH2:9]3)[C:14]1=[O:15]

Participants

3

Reactant 2

HCID 8623o-Toluenesulfonyl chlorideHCID 673028822-(Adamantan-2-yl)-4,4-dimethyl-1,2-diazetidin-3-one

Product 1

HCID 59361407HCID 59361407, compound

Procedure

2-(Adamantan-2-yl)-4,4-dimethyl-1,2-diazetidin-3-one and o-toluenesulfonyl chloride were used for a similar reaction and treatment as Example 169, and the title compound was obtained as a white crystalline powder.

Sources & evidence

ORD record
ord-24d2c4c0b41047f29c2c30d077e0b7ca
Source dataset
uspto-grants-2012_08
Patent number
US08252781B2

Reaction notes

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