HCID 59361533, compound → HCID 46194510, compound

Participants

Reaction Steps

A solution of 4,4-dimethyl-1-[(2E)-3-phenylprop-2-en-1-yl]-2-(adamantan-2-yl)-1,2-diazetidin-3-one (30.0 mg, 0.0860 mmol) prepared in Example 260 in ethyl acetate (2 mL) was added with 10% palladium carbon (catalyst amount), and under a hydrogen atmosphere the resultant was stirred at room temperature for 1 hour. The reaction solution was filtered using celite, concentrated in vacuo, and the title compound (24.3 mg, 80.2%) was obtained as a colorless oil.

Provenance & Evidence