HuagongsheHuagongshe Chemistry Print Report · For research reference only
1-Bromo-5-methanesulfonyl-2-methyl-3-nitro-benzene → 4-Bromo-6-methanesulfonyl-1H-indole
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 1-Bromo-5-methanesulfonyl-2-methyl-3-nitro-benzene | HCID 59151272 | — |
| Reactant | 4-bromo-1H-indole-6-sulfonic acid dimethylamide | HCID 59151342 | — |
| Product | 4-Bromo-6-methanesulfonyl-1H-indole | HCID 59151305 | — |
Reaction Steps
Prepared according to the method used in the preparation of 4-bromo-1H-indole-6-sulfonic acid dimethylamide using 1-bromo-5-methanesulfonyl-2-methyl-3-nitro-benzene in place of 3-bromo-4-N,N-trimethyl-5-nitro-benzenesulfonamide. The title compound was obtained as a white solid (1.8 g, 76%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08252792B2 |
| Source dataset | uspto-grants-2012_08 |
| ORD ID | ord-b44f4ca4826d4285aa5e4aa9f854e4ab |
| Source note | uspto-grants-2012_08 |