化工社化工社 化学情報印刷レポート · 研究参考用
1-Bromo-5-fluoro-2-methyl-3-nitrobenzene → 4-Bromo-6-fluoro-1H-indole
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | 1-Bromo-5-fluoro-2-methyl-3-nitrobenzene | HCID 2773385 | — |
| 反応物 | 4-bromo-1H-indole-6-sulfonic acid dimethylamide | HCID 59151342 | — |
| 生成物 | 4-Bromo-6-fluoro-1H-indole | HCID 24728173 | — |
反応手順
Prepared according to the method used in the preparation of 4-bromo-1H-indole-6-sulfonic acid dimethylamide using 1-bromo-5-fluoro-2-methyl-3-nitro-benzene in place of 3-bromo-4-N,N-trimethyl-5-nitro-benzenesulfonamide. The title compound was obtained as a white solid (6.06 g, 33%).
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US08252792B2 |
| 出典データセット | uspto-grants-2012_08 |
| ORD ID | ord-39a1186c9dde4a19b56ccaa3fe1d81a5 |
| 出典メモ | uspto-grants-2012_08 |