HuagongsheHuagongshe Chemistry Print Report · For research reference only
2-Methyl-1,3-dinitro-5-(trifluoromethyl)benzene → 6-(trifluoromethyl)-1H-indol-4-amine
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2-Methyl-1,3-dinitro-5-(trifluoromethyl)benzene | HCID 23568370 | — |
| Reactant | 4-bromo-1H-indole-6-sulfonic acid dimethylamide | HCID 59151342 | — |
| Product | 6-(trifluoromethyl)-1H-indol-4-amine | HCID 59333848 | — |
Reaction Steps
Prepared according to the method used in the preparation of 4-bromo-1H-indole-6-sulfonic acid dimethylamide using 2-methyl-1,3-dinitro-5-trifluoromethyl-benzene in place of 3-bromo-4,N,N-trimethyl-5-nitro-benzenesulfonamide. The title compound was obtained as a white solid (10.7 g, 99%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08252792B2 |
| Source dataset | uspto-grants-2012_08 |
| ORD ID | ord-936ef5b096e34651ab097dcdfc16f8be |
| Source note | uspto-grants-2012_08 |