HuagongsheHuagongshe Chemistry Print Report · For research reference only
2-Amino-5-methylthiazole → HCID 57927551, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2-Amino-5-methylthiazole | HCID 351770 | — |
| Reactant | Diphenylimidodicarboxylate | HCID 11043392 | — |
| Solvent | 1,4-Dioxane | HCID 31275 | — |
| Product | HCID 57927551 | HCID 57927551 | 93.6% |
Reaction Steps
A mixture of 2-amino-5-methylthiazole (2.0 g), diphenyl imidodicarbonate (CAS 99911-94-1) (4.5 g) and 1,4-dioxane (40 ml) was heated to reflux for 8 hours. After standing to cool, the precipitate was collected by filtration to obtain the title compound (3.00 g).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08252810B2 |
| Source dataset | uspto-grants-2012_08 |
| ORD ID | ord-491bf76431c946a9946cb8176effde71 |
| Source note | uspto-grants-2012_08 |