HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrazinecarboxylic acid, ethyl ester → HCID 178473566, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrazinecarboxylic acid, ethyl ester | HCID 20064 | — |
| Reactant | 4,5-Dihydro-2-(methylthio)thiazole | HCID 88324 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 178473566 | HCID 178473566 | 25.5% |
Reaction Steps
A mixture of ethyl carbazate (23.4 g), 2-(methylthio)-2-thiazoline (25 g) and ethanol (250 ml) was heated to reflux for 3 days. It was then stirred at room temperature for 2 days. The precipitate was collected by filtration and washed with ethanol to obtain the title compound (9.05 g).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08252810B2 |
| Source dataset | uspto-grants-2012_08 |
| ORD ID | ord-9e029b7850754c5e9764887691467095 |
| Source note | uspto-grants-2012_08 |