Thionyl Chloride → HCID 11550077, compound

HRID 889290Notes

Reaction equation

HRID 889290 reaction equation
[Cl:1][C:2]1[N:7]=[CH:6][C:5]([CH2:8]O)=[CH:4][C:3]=1[CH3:10].S(Cl)([Cl:13])=O>>[Cl:1][C:2]1[C:3]([CH3:10])=[CH:4][C:5]([CH2:8][Cl:13])=[CH:6][N:7]=1

Participants

3

Reactant 2

HCID 24386Thionyl ChlorideHCID 11686949(6-Chloro-5-methylpyridin-3-yl)methanol

Product 1

HCID 11550077HCID 11550077, compound

Procedure

The preparation is carried out analogously to Example 6A from 1.00 g (6.35 mmol) (6-chloro-5-methylpyridin-3-yl)methanol and 5 ml thionyl chloride. 1.26 g of the title compound, which is reacted without further purification, are obtained.

Sources & evidence

ORD record
ord-042e5a0fa4584e2386b55cb2eda523ab
Source dataset
uspto-grants-2012_08
Patent number
US08252817B2

Reaction notes

Loading…