HuagongsheHuagongshe Chemistry Print Report · For research reference only
Methanol → HCID 59186993, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Methanol | HCID 887 | — |
| Reactant | Sulfuric Acid | HCID 1118 | — |
| Reactant | HCID 59186979 | HCID 59186979 | — |
| Product | HCID 59186993 | HCID 59186993 | — |
Reaction Steps
150 mg (531 μmol) of the compound from Example 41 are dissolved in 20 ml methanol, 1 ml concentrated sulfuric acid are added and the mixture is heated under reflux overnight. After cooling, the precipitate formed is filtered off with suction, washed with methanol and dried.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08252817B2 |
| Source dataset | uspto-grants-2012_08 |
| ORD ID | ord-69e6e206a5af4db69f83945f268ec4c1 |
| Source note | uspto-grants-2012_08 |